Basic Course on NMR spectroscopy
Organized by CERMAX
| When |
17 Jun, 2009 09:00 AM
to
19 Jun, 2009 06:00 PM |
|---|---|
| Where | ITQB |
| Add event to your calendar |
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Basic course on NMR spectroscopy
Program:
17th of June
9.00 – Introduction to NMR spectroscopy (the phenomenon, basic properties of the signal).
10.00 – Instrumental aspects of the spectrometer.
10.30 – Break
11.00 – Introduction to TopSpin software.
13.00 – Lunch break
14.30 – Practical sessions - Sample preparation / Acquisition (1D, presat, APT) / Processing and analyzing 1D
18th of June
9.00 – Practical aspects of acquisition and processing (acquisition parameters, pulse programs, 90º pulse and T1 determination).
10.00 – The Nuclear Overhauser Effect
10.30 – Break
11.00 – Introduction to 2D NMR spectroscopy (Homonuclear correlation)
12.00 – INEPT, HSQC and HMBC
13.00 – Lunch break
14.30 – Practical sessions - Acquisition (COSY, HSQC) / Processing and analyzing 2D
19th of June
9.00 – DOSY.
9.45 – Protein structure
10.30 – Break
11.00 – Assignment strategies in small molecules (tutorial and exercises)
13.00 – Lunch break
14.30 – Practical sessions - Acquisition exercises
Faculty:
Helena Matias
Manolis Matzapetakis
Patrick Groves
Pedro Lamosa
Structure:
A three day course with theoretical and practical sessions covering basic aspects of the technique and oriented towards both beginners and routine NMR users.
Topics:
Basic theoretical aspects of NMR. Introduction to the most commonly used 1D and 2D homonuclear and heteronuclear techniques. Data acquisition and processing with a “hands-on” approach.
Applications:
The course is open and free of charge, however the practical sessions are restricted to 12 students. To apply to this course please send an e-mail to lamosa@itqb.unl.pt stating your interest accompanied by a short CV. For PhD students the course will correspond to 1 ECTS.
