{"id":5211,"date":"2022-05-24T00:00:00","date_gmt":"2022-05-23T23:00:00","guid":{"rendered":"https:\/\/www.itqb.unl.pt\/uncategorised\/15th-cermax-practical-course-on-basic-nmr\/"},"modified":"2022-05-24T00:00:00","modified_gmt":"2022-05-23T23:00:00","slug":"15th-cermax-practical-course-on-basic-nmr","status":"publish","type":"post","link":"https:\/\/www.itqb.unl.pt\/pt-pt\/sem-categoria\/15th-cermax-practical-course-on-basic-nmr\/","title":{"rendered":"15th CERMAX practical course on basic NMR"},"content":{"rendered":"\n

The 15th edition of the Basic course on NMR spectroscopy will take place from the 4th to the 8th of July.<\/strong><\/p>\n\n

This is a four and a half day course with theoretical and practical sessions<\/strong> covering basic aspects of the technique and oriented towards both beginners and routine NMR users.<\/p>\n\n

It will cover basic theoretical aspects of NMR; an introduction to the most commonly used 1D and 2D homonuclear and heteronuclear techniques; and data acquisition and processing with a \u201chands-on\u201d approach.<\/p>\n\n

The course is open and free of charge for NMR network member<\/strong>s, however the practical sessions are restricted to 12 students. To apply to this course please send an email to lamosa@itqb.unl.pt<\/strong> stating your interest\/reasons to attend until the 24th of June<\/strong>.<\/p>\n\n

 <\/p>\n\n

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 <\/p>\n\n

 <\/p>\n\n

Programme: <\/strong><\/p>\n\n

4th of July:<\/u><\/p>\n\n

14.00 \u2013 Introduction to NMR spectroscopy. (PL – Room 3.20)<\/em><\/span><\/p>\n\n

15.30 \u2013 Break<\/p>\n\n

15.50 \u2013 Instrumental aspects of the spectrometer \/Rules for spectrometer use. (HM – Room 3.20)<\/em><\/span><\/p>\n\n

16.30 \u2013 Spectrometer Guided tour and sample preparation. (HM – NMR Lab)<\/em><\/span><\/p>\n\n

 <\/p>\n\n

5th of July<\/u><\/p>\n\n

9.30 \u2013 1D Acquisition and processing. (PL – Room 3.20)<\/em><\/span><\/p>\n\n

10.15\u2013  Introduction to 2D NMR spectroscopy. (Homonuclear correlation). (PL – Room 3.20)<\/em><\/span><\/p>\n\n

11.00 \u2013 Break<\/p>\n\n

11.30 \u2013 The Nuclear Overhauser Effect. (ROL  – Room 3.20)<\/em><\/span><\/p>\n\n

12.30 \u2013 Lunch break<\/p>\n\n

14.00 \u2013 Heteronuclear correlation for small molecule. (PL  -Room 3.20)<\/span><\/em><\/p>\n\n

15.00 \u2013 Protein assignment and structure. (PL – Room 3.20)<\/em><\/span><\/p>\n\n

 <\/p>\n\n

6th of July<\/u><\/p>\n\n

9.30 \u2013 The paramagnetic effect and metalloproteins. (ROL – Room 3.20)<\/span><\/em><\/p>\n\n

10.15 \u2013 Residual Dipolar Couplings and disordered proteins. (TC – Room 3.20)<\/em><\/span><\/p>\n\n

11.00 \u2013 Break<\/p>\n\n

11.15 \u2013 Practical session I (PL, HM, LG, TC – NMR Spect and WS)<\/em><\/span><\/p>\n\n

Acquisition (1D, presat, p90, APT)<\/p>\n\n

Processing and analyzing 1D<\/p>\n\n

13.30 \u2013 Lunch break<\/p>\n\n

14.30 \u2013 Practical sessions I (cont). (PL, HM, LG, TC)<\/em><\/span><\/p>\n\n

 <\/p>\n\n

7th of July<\/u><\/p>\n\n

9.30 \u2013 NMR and Metabolomics\/ Quantitative NMR. (LG – Room 3.20)<\/em><\/span><\/p>\n\n

11.00 \u2013 Break<\/span><\/p>\n\n

11.15 \u2013 Practical session II (PL, HM, LG, TC)<\/em><\/span><\/p>\n\n

Acquisition (COSY, HSQC)<\/p>\n\n

Processing and analyzing 2D (NMR Spect and WS)<\/p>\n\n

13.30 \u2013 Lunch break<\/p>\n\n

14.30 \u2013 Practical sessions II (cont). (PL, HM, LG, TC)<\/span><\/em><\/p>\n\n

 <\/p>\n\n

8th of July<\/u><\/p>\n\n

9.30 \u2013 Assignment strategies in small molecules (tutorial and exercises). (PL – Room 3.20)<\/em><\/span><\/p>\n\n

10.45 \u2013 Break<\/p>\n\n

11.15 \u2013 Assignment strategies (cont). (PL  – Room 3.20)<\/em><\/span><\/p>\n\n

13.00 \u2013 Lunch break<\/p>\n\n

14.00 \u2013 Practical session III (PL, HM)<\/em><\/span><\/p>\n\n

Acquisition exercises (NMR Spect and WS)<\/p>\n\n

 <\/p>\n\n

Faculty:<\/strong><\/p>\n\n

Lu\u00eds Gafeira (LG)<\/p>\n\n

Helena Matias (HM)<\/p>\n\n

Pedro Lamosa (PL)<\/p>\n\n

Ricardo Louro (ROL)<\/p>\n\n

Tiago Cordeiro (TC)<\/p>\n\n

 <\/p>\n","protected":false},"excerpt":{"rendered":"

The 15th edition of the Basic course on NMR spectroscopy will take place from the 4th to the 8th of July. This is a four and a half day course with theoretical and practical sessions covering basic aspects of the technique and oriented towards both beginners and routine NMR users. It will cover basic theoretical aspects of NMR; an introduction to the most commonly used […]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":"","_members_access_role":[],"_members_access_error":""},"categories":[],"tags":[],"class_list":["post-5211","post","type-post","status-publish","format-standard","hentry"],"acf":[],"_links":{"self":[{"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/posts\/5211","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/comments?post=5211"}],"version-history":[{"count":0,"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/posts\/5211\/revisions"}],"wp:attachment":[{"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/media?parent=5211"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/categories?post=5211"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.itqb.unl.pt\/pt-pt\/wp-json\/wp\/v2\/tags?post=5211"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}