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[Course] 9th CERMAX practical course on basic NMR

When 21 Jun, 2016 09:00 AM to
24 Jun, 2016 06:00 PM
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Course topics include basic theoretical aspects of NMR, introduction to the most commonly used 1D and 2D homonuclear and heteronuclear techniques, and data acquisition and processing with a “hands-on” approach.

The course is open and free of charge for NMR network members, however the practical sessions are restricted to 12 students. To apply to this course please send an e-mail to lamosa@itqb.unl.pt stating your interest accompanied by a short CV until the 15 of June.

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Program

21st of June
9.30 Introduction to NMR spectroscopy PL Room 3.20
11.00 Break  
11.30 Instrumental aspects of the spectrometer
/Rules for spectrometer use.		 HM Room 3.20
12.15 1D Acquisition and processing PL Room 3.20
13.00 Lunch break  
14.00 NMR and Metabolomics/ Quantitative NMR GG Room 3.20
15.30 Break  
15.50 Spectrometer Guided tour and sample preparation HM NMR Lab

22nd of June
9.30 Introduction to 2D NMR spectroscopy (Homonuclear correlation) PL Room 3.20
10.15 The Nuclear Overhauser Effect ROL Room 3.20
11.00 Break  
11.15

Practical session I    
Acquisition (1D, presat, p90, APT)     
Processing and analyzing 1D (NMR Spect and WS)

 PL, HM, MM, IS
13.30 Lunch break  
14.30 Practical sessions I (cont) PL, HM, MM, IS

23rd of June
9.30 Heteronuclear correlation for small molecule and protein assignment MM Room 3.20
10.15 The paramagnetic effect and metalloproteins ROL Room 3.20
10.45 Break  
11.15 Practical session II   
Acquisition (COSY, HSQC)                           Processing and analyzing 2D (NMR Spect and WS)  		 PL, HM, MM, IS
13.30 Lunch break  
14.30 Practical sessions II (cont) PL, HM, MM, IS

24th of June
9.30 Assignment strategies in small molecules
(tutorial and exercises)		 PL Room 3.20
10.45 Break  
11.15 Assignment strategies (cont)  PL Room 3.20
13.00 Lunch break  
14.00 Practical session III  
Acquisition exercises (NMR Spect and WS)		 PL, HM

      
 

Faculty:

  • Gonçalo Graça
  • Helena Matias
  • Ivo Saraiva
  • Manolis Matzapetakis
  • Pedro Lamosa
  • Ricardo Louro

 

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