15th CERMAX practical course on basic NMR
Basic course on NMR spectroscopy
| When |
04 Jul, 2022 02:00 PM
to
08 Jul, 2022 04:00 PM |
|---|---|
| Contact Name | Pedro Lamosa |
| Add event to your calendar |
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Structure:
A four and a half day course with theoretical and practical sessions covering basic aspects of the technique and oriented towards both beginners and routine NMR users.
Topics:
Basic theoretical aspects of NMR. Introduction to the most commonly used 1D and 2D homonuclear and heteronuclear techniques. Data acquisition and processing with a “hands-on” approach.
Applications:
The course is open and free of charge for NMR network members, however the practical sessions are restricted to 12 students. To apply to this course please send an e-mail to lamosa@itqb.unl.pt stating your interest/reasons to attend until the 24th of June.
Programme:
4th of July:
14.00 – Introduction to NMR spectroscopy. (PL - Room 3.20)
15.30 – Break
15.50 – Instrumental aspects of the spectrometer /Rules for spectrometer use. (HM - Room 3.20)
16.30 – Spectrometer Guided tour and sample preparation. (HM - NMR Lab)
5th of July
9.30 – 1D Acquisition and processing. (PL - Room 3.20)
10.15– Introduction to 2D NMR spectroscopy. (Homonuclear correlation). (PL - Room 3.20)
11.00 – Break
11.30 – The Nuclear Overhauser Effect. (ROL - Room 3.20)
12.30 – Lunch break
14.00 – Heteronuclear correlation for small molecule. (PL -Room 3.20)
15.00 – Protein assignment and structure. (PL - Room 3.20)
6th of July
9.30 – The paramagnetic effect and metalloproteins. (ROL - Room 3.20)
10.15 – Residual Dipolar Couplings and disordered proteins. (TC - Room 3.20)
11.00 – Break
11.15 – Practical session I (PL, HM, LG, TC - NMR Spect and WS)
Acquisition (1D, presat, p90, APT)
Processing and analyzing 1D
13.30 – Lunch break
14.30 – Practical sessions I (cont). (PL, HM, LG, TC)
7th of July
9.30 – NMR and Metabolomics/ Quantitative NMR. (LG - Room 3.20)
11.00 – Break
11.15 – Practical session II (PL, HM, LG, TC)
Acquisition (COSY, HSQC)
Processing and analyzing 2D (NMR Spect and WS)
13.30 – Lunch break
14.30 – Practical sessions II (cont). (PL, HM, LG, TC)
8th of July
9.30 – Assignment strategies in small molecules (tutorial and exercises). (PL - Room 3.20)
10.45 – Break
11.15 – Assignment strategies (cont). (PL - Room 3.20)
13.00 – Lunch break
14.00 – Practical session III (PL, HM)
Acquisition exercises (NMR Spect and WS)
Faculty:
Luís Gafeira (LG)
Helena Matias (HM)
Pedro Lamosa (PL)
Ricardo Louro (ROL)
Tiago Cordeiro (TC)
