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[Course] 6th CERMAX practical course on basic NMR

When 24 Jun, 2013 09:00 AM to
27 Jun, 2013 06:00 PM
Where ITQB
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6th CERMAX practical course on basic NMR

The course is open and free of charge for NMR network members but practical sessions are restricted to 12 students. To apply please send an e-mail to lamosa@itqb.unl.pt stating your interest accompanied by a short CV.
 

Program

24th of June
9.30 Introduction to NMR spectroscopy (the phenomenon, basic properties of the signal)
10.30 Instrumental aspects of the spectrometer /Rules for spectrometer use.
11.00 Break
11.30 Introduction to TopSpin software
12.00 1D Acquisition and processing
13.00 Lunch break
14.00 NMR and Metabolomics/ Quantitative NMR
15.30 Break
16.00 Spectrometer Guided tour and sample preparation
   
25th of June
9.30 Introduction to 2D NMR spectroscopy (Homonuclear correlation)
10.15 INEPT, HSQC and HMBC
11.00 Break
11.30 Practical session I
  Acquisition (1D, presat, p90, APT) Processing and analyzing 1D
13.30 Lunch break
14.30 Practical sessions I (cont)
   
26th of June
9.00 The Nuclear Overhauser Effect
9.45 The paramagnetic effect and metalloproteins
10.30 Break
11.00 Protein structure
11.45 Practical session II
  Acquisition (COSY, HSQC) Processing and analyzing 2D
13.30 Lunch break
14.30 Practical sessions II (cont)
   
27th of June
10.00 Assignment strategies in small molecules (tutorial and exercises)
 11.00 Break
 11.30 Assignment strategies (cont)
 13.00 Lunch break
14.00 Practical session III
  Acquisition exercises


 
Faculty

  • Helena Matias
  • Ivo Saraiva
  • Luís Gafeira
  • Manolis Matzapetakis
  • Pedro Lamosa
  • Ricardo Louro
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